期刊论文

Li, X.J.

中文

中药材

1001-4454

2012

35

11

1782-1784

10.13863/j.issn1001-4454.2012.11.023

湖南省教育厅资助项目

本校为第一机构

目的:研究海南大风子叶的化学成分。方法:采用硅胶柱层析和SephadexLH-20凝胶柱层析进行分离纯化,通过理化性质和波谱数据分析进行结构鉴定。结果:从海南大风子叶的乙酸乙酯浸膏中分离了9个化合物,分别鉴定为:粘霉烯醇(I)、羊齿烯醇(Ⅱ)、羽扇豆醇(Ⅲ)、a-香树素(Ⅳ)、2,9-二甲基-2,8-葵二烯(V)、植烯(Ⅵ)、植醇(Ⅶ)、3,7,11,15-四甲基-1,2-十六烷二醇(Ⅷ)、3,5-二甲氧基-4-羟基苯甲醛(Ⅸ)。结论:所有化合物均为首次从该植物中分离得到。

OBJECTIVE: To study the chemical constituents from the leaf of Hydnocarpus hainanensis. METHODS: Compounds were isolated and purified by silica gel and Sephadex LH-20 column chromatography, their structures were identified by spectroscopic analysis. RESULTS: Nine compounds were isolated and identified as glutinol (I), fernenol (II), lupeol (III), a-armyrin (IV), 2, 9-dimethyldeca-2, 8-diene (V), phytenal (VI), phytol (VII), 3, 7, 11,15-tetramethylhexadecane-1,2-diol ( VI), 3, 5-dimethoxy-4-hydroxybenzaldehyde (IX). CONCLUSION: All the...