Development and validation of a UPLC–ELSD method for fast simultaneous determination of five bile acid derivatives in Calculus Bovis and its medicinal preparations

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成果类型：

期刊论文

作者：

Kong, Weijun;Jin, Cheng;Liu, Wei;Xiao, Xiaohe*;Zhao, Yanling;...

通讯作者：

Xiao, Xiaohe

作者机构：

[Kong, Weijun; Liu, Wei; Xiao, Xiaohe; Zhao, Yanling; Jin, Cheng; Zhang, Ping; Li, Xingfeng] 302 Mil Hosp China, China Mil Inst Chinese Mat Med, Beijing 100039, Peoples R China.

[Kong, Weijun; Li, Zulun] Chengdu Univ Tradit Chinese Med, Coll Pharm, Chengdu 610075, Peoples R China.

[Liu, Wei] Jiangxi Univ Tradit Chinese Med, Coll Pharm, Nanchang 330004, Peoples R China.

[Li, Xingfeng] Hunan Univ Tradit Chinese Med, Coll Pharm, Changsha 410208, Hunan, Peoples R China.

通讯机构：

[Xiao, Xiaohe] 3

302 Mil Hosp China, China Mil Inst Chinese Mat Med, Beijing 100039, Peoples R China.

语种：

英文

关键词：

Bile acid derivatives;Calculus Bovis;Method validation;Quantitative determination;UPLC-ELSD

期刊：

Food Chemistry

ISSN：

0308-8146

年：

2010

卷：

120

期：

页码：

1193-1200

DOI：

10.1016/j.foodchem.2009.11.064

基金类别：

Foundation of State Youth Science [30625042]; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [30600824]; [2009ZXJ0904-057]

机构署名：

本校为其他机构

院系归属：

药学院

摘要：

A reverse phase ultra-performance liquid chromatography coupled with evaporative light scattering detection (UPLC-ELSD) method was successfully established for simultaneous determination of five bile acid derivatives in Calculus Bovis and its medicinal preparations using a Waters Acquity UPLC T3 C18 column (2.1 × 50 mm, 1.8 μm) with gradient elution of 0.2% aqueous formic acid and acetonitrile. The influence of liquid flow-rate and column temperature, gas flow-rate and drift tube temperature on resolution was investigated to get the optimized...

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Development and validation of a UPLC–ELSD method for fast simultaneous determination of five bile acid derivatives in Calculus Bovis and its medicinal preparations

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