[蔡萍; 张水寒; 袁清照] Key Laboratory of Chinese Materia Medica Research and Development, Hunan Academy of Chinese Medicine, Changsha 410013, China
Key Laboratory of Modernization of Chinese Medicine, Hunan University of Chinese Medicine, Changsha 410208, China
[李顺祥; 黄丹] Key Laboratory of Chinese Materia Medica Research and Development, Hunan Academy of Chinese Medicine, Changsha 410013, China, Key Laboratory of Modernization of Chinese Medicine, Hunan University of Chinese Medicine, Changsha 410208, China
通讯机构:
[Yuan, Q.-Z.] K
Key Laboratory of Chinese Materia Medica Research and Development, Hunan Academy of Chinese Medicine, China
Objective To establish the HPLC fingerprint of Evodiae Fructus from genuine medicinal materials. Methods The gradient elution was adopted with acetonitrile 0. 04% octane sulfuric acid sodium salt and 0. 05% phosphoric acid in water as mobile phase, and detection wavelength was at 230 nm. All the samples were recorded in 80 min. Results The constitutents of Evodiae Fructus were well separated on HPLC, and the HPLC fingerprint of 11 batches of samples was established. The results showed that this method had a good repeatability, and the 21 common peaks had exclusive properties. Conclusion The me...