An Efficient and Modular Route to C-3*-TunePhos-Type Ligands

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成果类型：

期刊论文

作者：

Deng, Xu;Guan, Yu-Qing;Huo, Ning-Ning;Wang, Ya-Jing;Lv, Hui*;...

通讯作者：

Lv, Hui;Zhang, Xu-Mu

作者机构：

[Deng, Xu; Zhang, Xu-Mu; Lv, Hui; Zhang, XM; Guan, Yu-Qing; Huo, Ning-Ning] Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Hubei, Peoples R China.

[Deng, Xu] Cent S Univ, Coll Xiangya Pharmaceut Sci, Changsha 410013, Hunan, Peoples R China.

[Wang, Ya-Jing] Hunan Univ Chinese Med, Changsha 410208, Hunan, Peoples R China.

[Zhang, Xu-Mu] South Univ Sci & Technol China, Dept Chem, Shenzhen 518055, Peoples R China.

通讯机构：

[Lv, H; Zhang, XM] W

[Zhang, Xu-Mu] S

Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Hubei, Peoples R China.

South Univ Sci & Technol China, Dept Chem, Shenzhen 518055, Peoples R China.

语种：

英文

关键词：

C3*;TunePhos;type ligands;modular route;oxidative coupling

期刊：

Synthesis

ISSN：

0039-7881

年：

2017

卷：

期：

页码：

3726-3730

DOI：

10.1055/s-0036-1588421

基金类别：

Wuhan University [203273463]; Ministry of Education of ChinaMinistry of Education, China; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21302193, 21372179, 21432007, 21402145]

机构署名：

本校为其他机构

摘要：

An efficient and modular synthetic route to the bidentate C3&lowast;-TunePhos was developed, which allowed tunable steric and electronic effects of the ligands. This novel chemical technology highlights a versatile C3&lowast;-dibromodiphenyl intermediate that was accomplished by in situ Grignard exchange and subsequent Cu(II)-mediated intramolecular oxidative radical coupling process. It is worth noting that this advanced intermediate not only could be easily prepared by a diverse array of C3&lowast;-TunePhos-type ligands, but also could be used to facile synthesis of other novel type of N,S-c...

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An Efficient and Modular Route to C-3*-TunePhos-Type Ligands

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