期刊论文

中文

食品与药品

1672-979X

2015

3

183-186

10.3969/j.issn.1672-979X.2015.03.009

本校为第一机构

目的：提高尿石通丸的质量标准。方法采用高效液相色谱法（HPLC），色谱柱为Agilent TC C18，流动相为甲醇-水（37：63），流速1.0 mL/min，检测波长272 nm，同时测定君药广金钱草中夏佛塔苷和枳实中橙皮苷的含量。结果夏佛塔苷在0.1637~1.800μg范围内线性关系良好，r=0.9994，平均加样回收率98.9%， RSD 1.0%；橙皮苷在0.1526~1.679μg范围内线性关系良好，r=0.9991，平均加样回收率98.0%，RSD 0.8%。结论本实验建立的方法具有专属、简便、准确、可重复的特点，增强了尿石通丸的质量可控性，提高了尿石通丸的质量标准。

Objective To improve the quality standard of Niaoshitong Pills.Methods An Agilent TC C18 column was used, with mobile phase of methanol- water (37:63). The flow rate was 1.0 mL/min and the detective wavelength was 272 nm. Schaftoside inDesmodii styracifolii herba and hesperidin inAurantii fructus immaturus were simultaneously determined.Results The linear range of schaftoside was 0.1637-1.800μg,r=0.9994, the average recovery was 98.9 %, withRSD of 1.0 %. The linear range of hesperidin was 0.1526-1.679μg, r=0.9991, the average recovery was 98....